I had bought me some new bottles of CA last May, and I stored them in a cardboard box over the winter. All was fine when I took them out this spring. I went to grab a bottle of my med. CA the other day and it was hard as a rock. Checked the rest of them and all my med. and thick CA bottles were hard as a rock. My thin CA bottles are just fine. Btw, my med. and thick CA bottles have never been opened. I have one used and one new bottle of thin CA and both are just fine. Very odd! These were Bob smith's brand and I've always used them in the past with no problems.